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Development of Pilot Size Process for Zeolite Y and Zsm-5 Production from Kankara Kaolin

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Description

Download Development of Pilot Size Process for Zeolite Y and Zsm-5 Production from Kankara Kaolin. Chemical Engineering students who are writing their projects can get this material to aid their research work.

Abstract

The successes recorded at the laboratory for the synthesis of zeolite Y and ZSM-5 using Kankara kaolin sourced from Katsina state, Nigeria as starting material necessitated the need for upscale of the production process.

This thesis focused on the development of three pilot-size production units and characterizing the products obtained from those units. Pilot size reactors for dealumination and production of zeolite Y and ZSM-5 were developed and test run. 

Manual means of the design were adopted; the materials of construction were carefully selected for the fabrication stage. The process of producing zeolite from kaolin involves kaolin beneficiation, calcination, dealumination, zeolite recipe preparation, and crystallization.

The capacity of the pilot size dealumination, zeolite Y, and ZSM-5 reactors was 2.5 kg, 2 kg, and 4 kg per run respectively. The reaction temperature and time for the production of zeolite Y were 100°C and 7 hours respectively.

Introduction

Industrialization remains a major factor in measuring the development of a nation because it reduces the volume of importation and strengthens the economy of the nation. Chemical transformation of raw materials to products is one of the key industrial processes aimed at meeting the ever-rising needs of the global teeming population.

 Catalysts play a central role in most of the chemical transformation process and contribute immensely to the reduction in process thermal energy requirement, process simplification, reduced processing time, and most often reduction in materials requirement, thereby increasing output quantity and quality; which translates to higher profitability. 

Scale-up has been usually explained as to how to design a pilot or industrial reactor able to replicate through a standard methodology the results obtained in the laboratory. Scaling up reactors is a fundamental step in the realization and optimization of industrial plants.

Nigeria, with a huge amount of oil reserves estimated to be about 3 7.2 billion barrels and the 13th-word producer of petroleum, with four refineries across the nation and a total processing capacity of 450,000 barrels per day consumes approximately 1600 tonnes of zeolite catalyst per day. 

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